Quantitative Macroscopic Analysis of Solvent Effects with Emphasis on Pericyclic and Solvolysis Reactions

Joseph J. Gajewski
Department of Chemistry
Indiana University



The response of the Claisen Rearrangement to solvents in a manner not unlike the solvolysis of tert-butyl chloride solvolysis required understanding of both reactions. A multiparameter equation utilizing the Kirkwood-Onsager function of dielectric constant, the Hildebrand cohesive energy density, and the free energies of transfer of chloride ion and potassium ion between bulk solvents to address specific hydrogen bond donation and basicity, respectively, has been applied to these and related reactions to assess changes in dipole moment, solvophobicity, and specific acidity and basicity requirements of ground and transition states. The bottom line is that the hydrophobic effect is an important contributor in both reactions, and in solvolysis reactions, solvent basicity or nucleophilicity appears to play no role.